HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 20077013, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 4-Chlorophenyl isothiocyanate | HCID 16480 | — |
| Reactant | 2-Amino-3-benzyloxypyridine | HCID 90334 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 20077013 | HCID 20077013 | — |
Reaction Steps
A stirring mixture of 2-amino-3-benzyloxy pyridine (5.37 g, 0.0268 mol) and 4-chlorophenylisothiocyanate (5 g, 0.0295 mol) in toluene (20 ml) was heated under reflux for 2 h. After allowing to cool, the solution was treated with ether, and the resulting solid filtered off, washed and dried. Yield 8.33 g (84%), m.p. 140°-143 ° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05409943 |
| Source dataset | uspto-grants-1995_04 |
| ORD ID | ord-f1da553ee2d947b89c05396b4a5db1ad |
| Source note | uspto-grants-1995_04 |