HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 20076927, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Benzonitrile, 4-isothiocyanato- | HCID 17626 | — |
| Reactant | 2-Amino-3-benzyloxypyridine | HCID 90334 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 20076927 | HCID 20076927 | — |
Reaction Steps
A stirring mixture of 2-amino-3-benzyloxy pyridine (5.68 g, 0.0284 mol) and 4cyanophenyl isothiocyanate (5 g, 0.0312 mol) in toluene (20 ml) was heated under reflux for 2 h. After allowing to cool, the solution was treated with ether, and the resulting solid filtered off, washed and dried. Yield 9.4 g (92%), m.p. 163°-165 ° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05409943 |
| Source dataset | uspto-grants-1995_04 |
| ORD ID | ord-6543e603af7f40f7be385385ac2387da |
| Source note | uspto-grants-1995_04 |