HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylmethyl 4-(2,3-dihydro-1H-inden-2-yl)-2-butenoate → HCID 10465518, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylmethyl 4-(2,3-dihydro-1H-inden-2-yl)-2-butenoate | HCID 54078263 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 10465518 | HCID 10465518 | 85.1% |
Reaction Steps
6.45 g (22.1 mmol) of benzyl-4-(indan-2-yl)-2-butenoate was dissolved in 120 ml of methanol, to which 0.6 g of 10% palladium on carbon was added and stirred vigorously for 2.5 hours in the stream of hydrogen. The catalyst was removed by filtration, the filtrate was condensed to obtain 3.84 g of crystalline 4-(indan-2-yl)butanoic acid. Yield: 85%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05409956 |
| Source dataset | uspto-grants-1995_04 |
| ORD ID | ord-c533f9fc83d5471ab0aa69b2bed35a84 |
| Source note | uspto-grants-1995_04 |