HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15290057, compound → HCID 15290058, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15290057 | HCID 15290057 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15290058 | HCID 15290058 | 79.4% |
Reaction Steps
1.95 g of [2-[(4-nitrophenyl)sulfonylaminomethyl)indan-5-yl]acetic acid obtained in Example 22 was dissolved in 50 ml of methanol and added with 200 mg of 10% palladium on carbon, followed by stirring for 2 hours in the stream of hydrogen gas. The catalyst was removed by filtration, the filtrate was condensed and the residue was recrystallized from ethanol to obtain 1.43 g of crystals. Yield: 79%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05409956 |
| Source dataset | uspto-grants-1995_04 |
| ORD ID | ord-9e5b84e7364a46a68f92bfd58ab1eccf |
| Source note | uspto-grants-1995_04 |