HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 20077546, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Allyl Mercaptan | HCID 13367 | — |
| Reactant | 18-Crown-6 | HCID 28557 | — |
| Reactant | 3-Fluoropyridine-2-sulfonamide | HCID 19957930 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 20077546 | HCID 20077546 | — |
Reaction Steps
33.2 g (0.24 mol) of potassium carbonate as well as 1.32 g (0.005 mol) of 18-crown-6 and 15.8 g (0.17 mol) of 80% allylmercaptan in 50 ml of acetonitrile are added to a solution, cooled to +5° C., of 17.62 g (0.1 mol) of 3-fluoropyridin-2-ylsulfonamide in 400 ml of acetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05410063 |
| Source dataset | uspto-grants-1995_04 |
| ORD ID | ord-97281074cd22435e96a3c9e35c1b664a |
| Source note | uspto-grants-1995_04 |