HuagongsheHuagongshe Chemistry Print Report · For research reference only
Indole → HCID 19791527, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Indole | HCID 798 | — |
| Reactant | (4-Fluorophenyl)hydrazine | HCID 69982 | — |
| Reactant | 9-Azabicyclo[3.3.1]nonan-3-one--hydrogen chloride (1/1) | HCID 19791523 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19791527 | HCID 19791527 | 74% |
Reaction Steps
This compound was prepared from 9-azabicyclo[3.3.1]nonan-3-one hydrochloride and 4-fluorophenylhydrazine by the Fischer indole synthesis as described in Example 1, Method A. The product was obtained as yellow crystals (74% yield), mp 200°-201° C. (from methylene chloride).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05250537 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-54fda50e2a9a46aab7bda45e782e2c64 |
| Source note | uspto-grants-1993_10 |