HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydracrylonitrile → 2-Cyanoethyl 3-oxobutanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydracrylonitrile | HCID 8011 | — |
| Reactant | 2,2,6-Trimethyl-4H-1,3-dioxin-4-one | HCID 79368 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | 2-Cyanoethyl 3-oxobutanoate | HCID 12360406 | — |
Reaction Steps
A mixture of 16.33 g (0.23 mole) of 3-hydroxy-propionitrile and 28.4 g (0.20 mole) of 2,2,6-trimethyl-1,3-dioxen-4-one in the presence of 0.1 ml of triethylamine is heated to 90°-100° C. for 4 hrs 30 mins.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05250543 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-f867b4015bbf4bb48277a737c0a9cdd3 |
| Source note | uspto-grants-1993_10 |