Hydrochloric Acid → HCID 20088026, compound

HRID 1655424Notes

Reaction equation

HRID 1655424 reaction equation
[CH3:1][C:2]([C:5]1[CH:10]=[C:9]([S:11][C@@H:12]2[CH2:16][CH2:15][CH2:14][C@H:13]2O)[CH:8]=[C:7]([C:18]([CH3:21])([CH3:20])[CH3:19])[C:6]=1[OH:22])([CH3:4])[CH3:3].[ClH:23]>>[Cl:23][CH:13]1[CH2:14][CH2:15][CH2:16][CH:12]1[S:11][C:9]1[CH:10]=[C:5]([C:2]([CH3:4])([CH3:3])[CH3:1])[C:6]([OH:22])=[C:7]([C:18]([CH3:21])([CH3:20])[CH3:19])[CH:8]=1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 15287672HCID 15287672, compound

Product 1

HCID 20088026HCID 20088026, compound

Procedure

The product of Example 7 (0.40 g, 0.0012 mole) was stirred with concentrated hydrochloric acid (5 ml) at room temperature for 20 hours. The solid was removed by filtration, washed with water and air dried to give the product as a white powder. The product was purified by silica gel chromatography to give a white solid. The structure was supported by NMR.

Workup

  1. customThe solid was removed by filtration
  2. washwashed with water and air
  3. customdried

Sources & evidence

ORD record
ord-0f9a21cc8e4e42369c92bde7a51f366e
Source dataset
uspto-grants-1993_10
Patent number
US05250567

Reaction notes

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