HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 19792060, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 178441093 | HCID 178441093 | — |
| Reactant | HCID 178498184 | HCID 178498184 | — |
| Product | HCID 19792060 | HCID 19792060 | — |
Reaction Steps
Methyl 6-n-butyl-2-hydroxypyrimidine-4-carboxylate (prepared as described by Z. Budesinsky and F. Roubinek in Collection Czechoslovak Chem Commun., 26, 2871-2885 (1991)) is refluxed with phosphorous oxychloride, as described by the same authors for the chlorination of methyl 6-methyl-2-hydroxypyrimidine-4-carboxylate, to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05250548 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-40bf8f79537944cfacfe579e70100c02 |
| Source note | uspto-grants-1993_10 |