HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 178441734, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 67884770 | HCID 67884770 | — |
| Reactant | HCID 178441730 | HCID 178441730 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 178441734 | HCID 178441734 | — |
Reaction Steps
2-n-Butyl-5-amino-4-{N-[N-methyl-(2'-(1H-tetrazol-5-yl]biphenyl-4-yl)methyl]amino}pyrimidine, the product of Example 46, is dissolved in chloroform containing triethylamine and treated with one equivalent of methanesulfonyl chloride to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05250548 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-3a6b6f441aa842c483492120e18502f8 |
| Source note | uspto-grants-1993_10 |