HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl ethylmalonate → HCID 19792074, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl ethylmalonate | HCID 8610 | — |
| Reactant | 2-Chloro-3-nitropyridine | HCID 79613 | — |
| Reactant | Sodium bis(trimethylsilyl)amide | HCID 2724254 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19792074 | HCID 19792074 | — |
Reaction Steps
Diethyl ethylmalonate is dissolved in tetrahydrofuran and treated with one equivalent of sodium bis(trimethylsilyl)amide followed by 2-chloro-3-nitropyridine to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05250548 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-0a4ce5da5d764fcdb3a463016abf605d |
| Source note | uspto-grants-1993_10 |