Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Chlorobenzimidazole → Hydrochloric Acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Chlorobenzimidazole | HCID 78572 | — |
| 반응물 | 1-Aminotetralin, (R)- | HCID 7058072 | — |
| 생성물 | Hydrochloric Acid | HCID 313 | — |
| 생성물 | NS-8593 | HCID 11587013 | — |
반응 단계
The title compound was prepared from 2-chlorobenzimidazole and (R)-1,2,3,4-tetrahydro-l-naphthylamine by Procedure A (40 min at 170° C.). The product was filtered off and washed with acetonitrile to give the title compound as a HCl salt (white solid, mp 264-265° C.). MS(ES+) m/z 264 ([M+1]30, 100).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07737167B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-20c8ebbf2dee4f958242e04dc6a1c9cc |
| 출처 메모 | uspto-grants-2010_06 |