Hydrochloric Acid → HCID 10923601, compound

Participants

Reaction Steps

To 6.7g of 1,7-diacetoxy-2,4,6-trinitro-2,4,6-triazaheptane (18.9 mmol) was added 33 ml of 30% aqueous HCl. The mixture was then stirred for 48 hours at room temperature. The solid was collected by suction filtration through a sintered glass funnel, washed with distilled water, and dried in vacuo. Collected was 3.9 g (75%); melting point 134°-138° C.; 1H NMR spectrum (d3 -acetonitrile): δ 5.40 and 5.87.

Provenance & Evidence