HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxybenzoic Acid → HCID 54140554, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxybenzoic Acid | HCID 135 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 2-Propoxypropan-1-ol | HCID 25055 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 54140554 | HCID 54140554 | 90% |
Reaction Steps
3.2 g of p-hydroxybenzoic acid and 13.8 g of optically active 2-methyl-2-propyloxyethanol were refluxed under heating together with 1 ml of sulfuric acid in benzene for 20 hours. The reaction liquid was condensed and purified by column chromatography to obtain 5.0 g (yield: 90 %) of the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05252251 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-645967e3bc8a4d978d94843e6b132937 |
| Source note | uspto-grants-1993_10 |