HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(1-Benzyl-1H-imidazol-2-yl)methanamine → HCID 136098640, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(1-Benzyl-1H-imidazol-2-yl)methanamine | HCID 13478011 | — |
| Reactant | HCID 136403346 | HCID 136403346 | — |
| Product | HCID 136098640 | HCID 136098640 | 21% |
Reaction Steps
Using the process described in Example 5, p-[N-(3,4-dihydro-2-methyl-4-oxoquinazolin-6-ylmethyl)-N-ethylamino]benzoyl azide was reacted with (1-benzylimidazol-2-yl)methylamine to give N-(1-benzylimidazol-2-yl)methyl-p-[N-(3,4-dihydro-2-methyl-4-oxoquinazolin-6-ylmethyl)-N-ethylamino]benzamide (containing 1.3 equivalents of water) in 21% yield, m.p. 217°-221° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05252573 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-97ca514854c0493e9214cdb0b9a4c722 |
| Source note | uspto-grants-1993_10 |