HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178501209, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | 2-Azabicyclo(2.2.2)octan-3-one | HCID 137887 | — |
| Product | HCID 178501209 | HCID 178501209 | — |
Reaction Steps
Dissolve 3-isoquinuclidone (1.5 g) in methanol (50 mL) and saturated with HCl. Let stand overnight then warm to reflux for 16 hours. Evaporate the solvent in vacuo to give cis-4-amino-cyclohexanecarboxylic acid, methyl ester hydrochloride as a white foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05252601 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-ae75fc8efa694404a5a1678f1c12694e |
| Source note | uspto-grants-1993_10 |