HRID1656053
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
Dissolve 3-isoquinuclidone (1.5 g) in methanol (50 mL) and saturated with HCl. Let stand overnight then warm to reflux for 16 hours. Evaporate the solvent in vacuo to give cis-4-amino-cyclohexanecarboxylic acid, methyl ester hydrochloride as a white foam.
WORKUP
后处理
- temperaturethen warm
- temperatureto reflux for 16 hours
- customEvaporate the solvent in vacuo