HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1656330Generated: November 1, 2026
1-(3-Chlorophenyl)piperazine → HCID 19787740, compound
https://huagongshe.com/reaction/1656330
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-(3-Chlorophenyl)piperazine | HCID 1355 | — |
| Reactant | HCID 19787778 | HCID 19787778 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 19787740 | HCID 19787740 | — |
Reaction Steps
Suspend 2 mmol (570 mg) of 6-chloro-5-benzyl-3-phenyl-1,2,4-triazine obtained in Step A of Example 57 in 40 ml of butanol, and add 4 equivalents of 1-(3-chlorophenyl)piperazine. Heat for 12 hours at 120° C., concentrate the solution, take up in ether, filter the resulting precipitate and recrystallise it from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05254548 |
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| Source dataset | uspto-grants-1993_10 |
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| ORD ID | ord-33c3503bd86b4e54900d75e5ca4bc981 |
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| Source note | uspto-grants-1993_10 |
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