HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allylamine → HCID 178457519, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allylamine | HCID 7853 | — |
| Reactant | Benzenecarboximidic acid, ethyl ester, hydrochloride (1:1) | HCID 79249 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178457519 | HCID 178457519 | — |
Reaction Steps
To a solution of ethyl benzimidate hydrochloride (20 g) in methanol at 0° C. was added allyl amine. The resulting solution was allowed to stand for 2 days at 5° C. before it was evaporated to yield a solid which was collected and washed with ether to give N-allyl benzamidine hydrochloride (21.5 g) as a white solid; 300 MHz NMR: 10.1 (s,1), 9.68 (s,1), 9.29 (s,1), 7.72 (s,5), 5.92 (m,1), 5.35 (d,2), 5.26 (d,2), 4.14 (s,2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05254558 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-25773a2f389f4d819f3d691f63b78d12 |
| Source note | uspto-grants-1993_10 |