3-Cyanopyridine → HCID 12218258, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of ethanol (200 mL) in chloroform (100 mL) at 0° C. was added acetyl chloride (190 mL) and a solution of 3-cyanopyridine (25 g) in (300 mL) of chloroform. The solution was allowed to warm to 25° C. and to stand for 1 day. A white solid separated from solution. The solvent was removed and the white solid collected and washed with ether to provide pure ethyl 3-pyridine-carboximidate hydrochloride as a white solid; MS: m/z=152(M+1).

Provenance & Evidence