Aminoacetaldehyde dimethyl acetal → HCID 178495959, compound

HRID 1656529Notes

Reaction equation

HRID 1656529 reaction equation
Cl.[N:2]1[CH:7]=[CH:6][CH:5]=[C:4]([C:8](=[NH:12])OCC)[CH:3]=1.[CH3:13][O:14][CH:15]([O:18][CH3:19])[CH2:16][NH2:17]>>[CH3:13][O:14][CH:15]([O:18][CH3:19])[CH2:16][NH:17][C:8]([C:4]1[CH:3]=[N:2][CH:7]=[CH:6][CH:5]=1)=[NH:12]

Participants

3

Reactant 2

HCID 89728Aminoacetaldehyde dimethyl acetalHCID 12218258HCID 12218258, compound

Product 1

HCID 178495959HCID 178495959, compound

Procedure

Ethyl 3-pyridinecarboximidate hydrochloride and aminoacetaldehyde dimethyl acetal were subjected to a procedure similar to that described in Example 8.b. to provide pure N-(2,2-dimethoxyethyl)-3-pyridinecarboxamidine as an oil; MS: m/z=210(M+1).

Sources & evidence

ORD record
ord-8f4d7dfe55ba47f7a7c3a295f4977b82
Source dataset
uspto-grants-1993_10
Patent number
US05254558

Reaction notes

Loading…