HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 10381261, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Dimethyl methoxymethylenemalonate | HCID 90770 | — |
| Reactant | HCID 178495959 | HCID 178495959 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 10381261 | HCID 10381261 | — |
Reaction Steps
Dimethyl methoxymethylenemalonate and N-(2,2-dimethoxy-ethyl) -3-pyridinecarboxamidine were subjected to a procedure similar to that described in Example 1.b. Chromatography, with methanol:diethyl ether (gradient, 0:100, 10:90) as the eluent, gave methyl 1-(2,2-dimethoxy-ethyl)-2-(3-pyridyl)pyrimidin-6(1H)-one-5-carboxylate as an oil; MS: m/z=320(M+1); TLC: Rf =0.4, methanol:diethyl ether (5:95).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05254558 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-f7d9fc97ff084dbb84915e2c0d6500d3 |
| Source note | uspto-grants-1993_10 |