HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 19787880, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | {2-(4-Nitro-phenyl)-6-oxo-1-[(3,3,3-trifluoro-1-isopropyl-2-oxo-propylcarbamoyl)-methyl]-1,6-dihydro-pyrimidin-5-yl}-carbamic acid benzyl ester | HCID 10415744 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19787880 | HCID 19787880 | — |
Reaction Steps
2-[5-Benzyloxycarbonylamino-2-(4-nitrophenyl)-6-oxo-1,6-dihydro-1-pyrimidinyl]-N-(3,3,3-trifluoro-1-isopropyl-2-oxopropyl)acetamide was subjected to a procedure similar to that described in Example 6 to give a brown solid; chromatography solvent: methanol:dichloromethane (gradient, 5:95, 10:90); NMR (DMSO/D2O): 7.29 (s,1), 7.01 (d,2), 6.49 (d,2), 4.52 (m,2), 4.10 (d,2), 2.25 (m,1), 0.88 (d,3), 0.80 (d,3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05254558 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-37d38ea397ef41d3b501ce755adeaa66 |
| Source note | uspto-grants-1993_10 |