Sulfuryl chloride → HCID 19787917, compound

HRID 1656539Notes

Reaction equation

HRID 1656539 reaction equation
Cl.[N+:2]([C:5]1[CH:12]=[CH:11][C:8]([CH2:9][NH2:10])=[CH:7][CH:6]=1)([O-:4])=[O:3].[S:13](Cl)([Cl:16])(=[O:15])=[O:14]>C(#N)C>[N+:2]([C:5]1[CH:6]=[CH:7][C:8]([CH2:9][NH:10][S:13]([Cl:16])(=[O:15])=[O:14])=[CH:11][CH:12]=1)([O-:4])=[O:3]

Participants

4

Reactant 2

HCID 24648Sulfuryl chlorideHCID 112524674-Nitrobenzylamine hydrochloride

Product 1

HCID 19787917HCID 19787917, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

The intermediate 4-nitrobenzylaminosulfonyl chloride was prepared from 4-nitrobenzylamine hydrochloride and sulfuryl chloride at reflux in acetonitrile. The solvent was evaporated and the crude material used without further purification.

Workup

  1. customThe solvent was evaporated
  2. customthe crude material used without further purification

Sources & evidence

ORD record
ord-942b48ef38684993ae7198e978b34f27
Source dataset
uspto-grants-1993_10
Patent number
US05254558

Reaction notes

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