HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuryl chloride → HCID 19787917, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | 4-Nitrobenzylamine hydrochloride | HCID 11252467 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 19787917 | HCID 19787917 | — |
Reaction Steps
The intermediate 4-nitrobenzylaminosulfonyl chloride was prepared from 4-nitrobenzylamine hydrochloride and sulfuryl chloride at reflux in acetonitrile. The solvent was evaporated and the crude material used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05254558 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-942b48ef38684993ae7198e978b34f27 |
| Source note | uspto-grants-1993_10 |