HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 15676484, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Acetate | HCID 517044 | — |
| Reactant | 4-Bromomethyl-2-phenyl-benzothiazole | HCID 15676483 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 15676484 | HCID 15676484 | — |
Reaction Steps
53 g (0.176 mol) of the compound from Example I and 20 g (0.2 mol) of potassium acetate were stirred at room temperature in 500 ml of dimethylformamide for 24 h, the solvent was stripped off in vacuo, water was added, and the product was filtered off with suction and dried. Yield: 46 g (92% of theory) M.p. 83°-84° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05254692 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-bb6fb434361044ecbdec535f4dd75711 |
| Source note | uspto-grants-1993_10 |