HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lawesson's reagent → HCID 15676488, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lawesson's reagent | HCID 87949 | — |
| Reactant | HCID 15676487 | HCID 15676487 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 15676488 | HCID 15676488 | — |
Reaction Steps
98 g (0.4 mol) of the compound from Example V and 162 g (0.4 mol) of Lawesson's reagent were boiled in 1 l of toluene overnight, and the mixture was concentrated and purified on SiO2 (cyclohexane/ethyl acetate=8:2) Yield: 93 g (80% of theory) as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05254692 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-d752d943e0c74f4ea128873e1cf308f0 |
| Source note | uspto-grants-1993_10 |