HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminum hydride → 7-Hydroxymethyl-2-phenyl-benzoxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminum hydride | HCID 14487 | — |
| Reactant | 7-Benzoxazolecarboxylic acid, 2-phenyl-, methyl ester | HCID 19939918 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 7-Hydroxymethyl-2-phenyl-benzoxazole | HCID 19939919 | — |
Reaction Steps
10 mmol of the compound from Example XV were dissolved in 50 ml of toluene, then 40 ml of DIBAH*(20% strength in toluene) were added at 0° C. and the mixture
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05254692 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-f3d6f396151349c5ac4772a46dfc1bdb |
| Source note | uspto-grants-1993_10 |