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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1656695Generated: November 1, 2026

Delta-Valerolactone → 5-Hydroxypentanoic Acid SodiuM Salt

https://huagongshe.com/reaction/1656695

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDelta-ValerolactoneHCID 10953—
ReactantSodium HydroxideHCID 14798—
Product5-Hydroxypentanoic Acid SodiuM SaltHCID 23695195—

Reaction Conditions

Temperature65 °C

Reaction Steps

A suspension of 800 mg (8.0 mmol) of δ-valerolactone in 8 mL (8.0 mmol, 1.0 equiv) of 1N aqueous sodium hydroxide was heated at 65° C. overnight. The clear solution was cooled and concentrated. Toluene was added and the resultant slurry was concentrated to give a white solid: IR (nujol mull) 1550 cm-1.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05254682
Source datasetuspto-grants-1993_10
ORD IDord-7853824dc11f4748987e8aabf2be3729
Source noteuspto-grants-1993_10