HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 20083141, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 54253840 | HCID 54253840 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20083141 | HCID 20083141 | 75.4% |
Reaction Steps
100 mg of the compound (163) obtained in Example 40 and 1.4 ml of triethylamine were added to 5 ml of ethanol, and the solution was heated at reflux for 15.5 hours. After air-cooling, the solids were filtered and washed successively with ethanol and ether to obtain 65 mg of the subject compound (164).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05254685 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-809476f831124197b9d59366b799f45d |
| Source note | uspto-grants-1993_10 |