HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 19788688, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | (Diethylamino)sulfur trifluoride | HCID 123472 | — |
| Reactant | HCID 20083158 | HCID 20083158 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19788688 | HCID 19788688 | — |
Reaction Steps
65 mg of the compound (177) obtained in Example 54 was suspended in 5 ml of tetrahydrofuran, and 270 μl of diethylaminosulfurtrifluoride was added to the solution. The solution was stirred for 4 hours, and 1 ml of ethanol was added to the solution. The deposited solid matter was filtered off and washed with ether to obtain 28 mg of the subject compound (181).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05254685 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-c7f0c41d26c34736ad1863408fe0207a |
| Source note | uspto-grants-1993_10 |