Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | HCID 20083130 | HCID 20083130 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 20083096 | HCID 20083096 | — |
Reaction Steps
4 mg of the compound (202) obtained in Example 73 and 10 μl of pyrrolidine were added to 1 ml of acetonitrile, and the solution was heated at 80° C. for 3 hours. After air-cooling, the solvent was removed by distillation, and the residue was filtered off and washed with ethanol and ether in this order to obtain 2 mg of the subject compound (203).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05254685 |
|---|
| Source dataset | uspto-grants-1993_10 |
|---|
| ORD ID | ord-1404daf568254b2e82917884e5493074 |
|---|
| Source note | uspto-grants-1993_10 |
|---|
