Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Nitromethane | HCID 6375 | — |
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 3-Pyridinecarboxaldehyde | HCID 10371 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12021882 | HCID 12021882 | — |
Reaction Steps
To a cooled stirring solution of 15 grams (0.25 mol) nitromethane and 0.35 gram (0.005 mol) diethylamine in 26 milliliters of ethanol was added dropwise 10 grams (0.093 mol) 3-pyridine carboxaldehyde. The reaction was stirred for 3 hours at 0° C. then warmed to ambient temperature. Concentration yielded crude 1-(3-pyridyl)-2-nitroethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05256626 |
|---|
| Source dataset | uspto-grants-1993_10 |
|---|
| ORD ID | ord-cd95e3b067e040b1ad052ccf62be70ef |
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| Source note | uspto-grants-1993_10 |
|---|
