HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → N-t-butyl-3,3-diphenylcyclopentylamine methanesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | N-t-butyl-3,3-diphenylcyclopentylamine | HCID 10379659 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | N-t-butyl-3,3-diphenylcyclopentylamine methanesulfonate | HCID 19787464 | 78.6% |
Reaction Steps
To a solution of N-t-butyl-3,3-diphenylcyclopentylamine (0.49 g) in chloroform and methanol was added a solution of methanesulfonic acid (0.16 g) in methanol. The solvent was evaporated in vacuo and ethyl acetate was added. After standing for 2 hours, the resulting precipitate was collected to give N-t-butyl-3,3-diphenylcyclopentylamine methanesulfonate (0.51 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05256824 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-45f3661f9d894fc58b90de7396b5e343 |
| Source note | uspto-grants-1993_10 |