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HRID1657288

反应详情

EQUATION

反应方程式

HRID 1657288 的结构方程式

REACTANTS

反应物

2
结构：CS(=O)(=O)O
HCID6395

Methanesulfonic acid

CH4O3S

结构：CC(C)(C)NC1CCC(c2ccccc2)(c2ccccc2)C1
HCID10379659

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)NC1CCC(c2ccccc2)(c2ccccc2)C1.CS(=O)(=O)O
HCID19787464

未命名化合物

收率 78.6%

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CO
溶剂HCID887

Methanol

CH4O

2 次

结构：ClC(Cl)Cl
溶剂HCID6212

Chloroform

CHCl3

PROCEDURE

实验过程

To a solution of N-t-butyl-3,3-diphenylcyclopentylamine (0.49 g) in chloroform and methanol was added a solution of methanesulfonic acid (0.16 g) in methanol. The solvent was evaporated in vacuo and ethyl acetate was added. After standing for 2 hours, the resulting precipitate was collected to give N-t-butyl-3,3-diphenylcyclopentylamine methanesulfonate (0.51 g).

WORKUP

后处理

  1. customThe solvent was evaporated in vacuo and ethyl acetate
  2. additionwas added
  3. customthe resulting precipitate was collected