HRID1657334

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID93700

2-(1-Chloroethyl)-1,4-dimethylbenzene

C10H13Cl

HCID5360545

Sodium

HCID178526253

未命名化合物

PRODUCTS

生成物

HCID501135

2-(1-[2,5-dimethylphenyl]-ethylthio)pyridine N-oxide

C15H17NOS

收率 83%

PROCEDURE

实验过程

The intermediate 2-(1-[2,5-dimethylphenyl]-ethylthio)pyridine N-oxide is prepared from 1-(2,5-dimethylphenyl)ethyl chloride and 2-mercaptopyridine N-oxide, sodium salt by the procedure described in Example 2. Melting point 118° - 120°C. Structure confirmed by IR and NMR.