HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-4-(1-chloroethyl)benzene → 2-{[1-(4-Bromophenyl)ethyl]sulfanyl}-1-oxo-1lambda~5~-pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-4-(1-chloroethyl)benzene | HCID 14557467 | — |
| Reactant | HCID 178507102 | HCID 178507102 | — |
| Product | 2-{[1-(4-Bromophenyl)ethyl]sulfanyl}-1-oxo-1lambda~5~-pyridine | HCID 54500435 | 85% |
Reaction Steps
The compound 2-(1-[4-bromophenyl]ethylthio)-pyridine N-oxide is prepared from 1-(4-bromophenyl)-ethylchloride and 2-mercaptopyridine N-oxide sodium salt by the procedure described in Example 1. The melting point is 113° - 115°C. Structure is confirmed by IR and NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03960542 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-ba60c4410fc7407296a8583a982810d1 |
| Source note | uspto-grants-1976_06 |