HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiourea → HCID 21533401, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiourea | HCID 2723790 | — |
| Reactant | HCID 21533367 | HCID 21533367 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21533401 | HCID 21533401 | — |
Reaction Steps
A solution of 6.3 g of thiourea in 300 ml of methanol is added to a solution of 25 g of 3-carboethoxy-4-chloro-6-cycloheptyl-quinoline in 200 ml of ethanol and the mixture is left to stand for 2 days at room temperature. The crude 3-carboethoxy-4-amidinothio-6-cycloheptyl-quinoline-hydrochloride formed, of melting point 280°C (decomposition), is then filtered off.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03960868 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-35b62f56ab834386ae87cfba4945cdf4 |
| Source note | uspto-grants-1976_06 |