HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromomethylnaphthalene → HCID 86733502, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromomethylnaphthalene | HCID 70320 | — |
| Reactant | HCID 54199631 | HCID 54199631 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 86733502 | HCID 86733502 | 99.1% |
Reaction Steps
7-(2-Hexyl)-2,2-dimethyl-4-(4-pyridyl)-2H-chromen-5-ol (5.00 g), 2-bromomethyl-naphthalene (3.54 g) and acetone (70 ml) were heated together under reflux for 6 hours. The resulting pale yellow precipitate was filtered and dried to yield 4-[7-(2-hexyl)-5-hydroxy-2,2-dimethyl-2H-chromen-4-yl]-1-(2-naphthylmethyl) pyridinium bromide (8.20 g) m.p. 236°- 239°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03960879 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-e49c9d11042e49dcaa7ffb439fa2d2b7 |
| Source note | uspto-grants-1976_06 |