HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 12274826, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | AC1Mcynq | HCID 2780821 | — |
| Product | HCID 12274826 | HCID 12274826 | — |
Reaction Steps
A suspension of 20 g of 9,10-dibromo-9,10-dihydro-4H-benzo[4,5]cyclohepta[1,2-b]thiophen-4-one in 400 cc of methanol is boiled at reflux for 5 hours. 9-Bromo-9,10-dihydro-10-methoxy-4H-benzo[ 4,5]cyclohepta[1,2-b]thiophen-4-one (M.P. 103°-106°) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03960894 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-93298ee647d64582871a273fa59fc4cf |
| Source note | uspto-grants-1976_06 |