HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Bicarbonate → sodium 7-methoxy-1-oxo-1H-2-benzothiopyran-3-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 7-methoxy-1-oxo-1H-2-benzothiopyran-3-carboxylic acid | HCID 21440742 | — |
| Solvent | Water | HCID 962 | — |
| Product | sodium 7-methoxy-1-oxo-1H-2-benzothiopyran-3-carboxylate | HCID 23666647 | — |
Reaction Steps
To a stirred suspension of 2.0347 g. (8.613 mM) of 7-methoxy-1-oxo-1H-2-benzothiopyran-3-carboxylic acid in 50 ml. of distilled water is added 0.7236 g. (8.613 mM) of sodium bicarbonate. The resulting mixture is stirred at 25°-35° for 1.25 hours, filtered, and the filtrate freeze-dried to give sodium 7-methoxy-1-oxo-1H-2-benzothiopyran-3-carboxylate as a pale yellow solid, m.p. >350°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03960892 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-a29111a5346149898d556cf6a9571d0b |
| Source note | uspto-grants-1976_06 |