HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Bicarbonate → sodium 4-methyl-1-oxo-1H-2-benzothiopyran-3-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 4-methyl-1-oxo-1H-2-benzothiopyran-3-carboxylic acid | HCID 21423681 | — |
| Solvent | Water | HCID 962 | — |
| Product | sodium 4-methyl-1-oxo-1H-2-benzothiopyran-3-carboxylate | HCID 23666645 | — |
Reaction Steps
To a stirred suspension of 2.0090 g. (9.122 mM) of 4-methyl-1-oxo-1H-2-benzothiopyran-3-carboxylic acid in 50 ml. of distilled water is added 0.7663 g. (9.122 mM) of sodium bicarbonate. After stirring at room temperature for 1.5 hours, the solution is filtered and the filtrate freeze-dried to give sodium 4-methyl-1-oxo-1H-2-benzothiopyran-3-carboxylate, m.p. 330° (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03960892 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-9b6f3ee43167472f945a7f437988a238 |
| Source note | uspto-grants-1976_06 |