Hydroxylamine → 6-Undecanone oxime

HRID 1657528Notes

Reaction equation

[CH3:1][CH2:2][CH2:3][CH2:4][CH2:5][C:6](=O)[CH2:7][CH2:8][CH2:9][CH2:10][CH3:11].[NH2:13][OH:14]>>[CH3:1][CH2:2][CH2:3][CH2:4][CH2:5][C:6](=[N:13][OH:14])[CH2:7][CH2:8][CH2:9][CH2:10][CH3:11]

Participants

Reactant 2

HCID 787Hydroxylamine

HCID 135616-Undecanone

Product 1

HCID 5519936-Undecanone oximeYield 80%

Procedure

Using the general procedure described in Sedgwick, Organic Chemistry of Nitrogen, pages 169-175 (1937 Edition), 1.2 moles of 6-undecanone is reacted with an alcohol solution of 1 mole of hydroxylamine at room temperature to produce 0.8 moles of 6-undecanone oxime, ##EQU1## contaminated with 3.5% 6-undecanone.

Sources & evidence

ORD record: ord-c1435e35ee754cf4927f0e1c636dd48e
Source dataset: uspto-grants-1976_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03960955

Reaction notes

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