3,4-Dichloroaniline → HCID 773317, compound

HRID 1657577Notes

Reaction equation

HRID 1657577 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:6]=[CH:7][C:8]=1[Cl:9])[NH2:5].[CH:10]1([N:16]=[C:17]=[S:18])[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11]1>>[CH:10]1([NH:16][C:17]([NH:5][C:4]2[CH:6]=[CH:7][C:8]([Cl:9])=[C:2]([Cl:1])[CH:3]=2)=[S:18])[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11]1

Participants

3

Reactant 2

HCID 72573,4-DichloroanilineHCID 14289Cyclohexyl isothiocyanate

Product 1

HCID 773317HCID 773317, compound

Procedure

A mixture of 16.2 gm. (0.1 mole) of 3,4-dichloroaniline and 14.1 gm. (0.1 mole) of cyclohexyl isothiocyanate is heated together on the steam bath for four hours. The solid is crystallized from ethanol-water; 18 gm. (59%), m.p. 159°-162°.

Workup

  1. additionA mixture of 16.2 gm
  2. customThe solid is crystallized from ethanol-water

Sources & evidence

ORD record
ord-35e7dfcb8fc44e49a873d439e4db30f9
Source dataset
uspto-grants-1976_06
Patent number
US03961056

Reaction notes

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