HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dichloroaniline → HCID 773317, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dichloroaniline | HCID 7257 | — |
| Reactant | Cyclohexyl isothiocyanate | HCID 14289 | — |
| Product | HCID 773317 | HCID 773317 | — |
Reaction Steps
A mixture of 16.2 gm. (0.1 mole) of 3,4-dichloroaniline and 14.1 gm. (0.1 mole) of cyclohexyl isothiocyanate is heated together on the steam bath for four hours. The solid is crystallized from ethanol-water; 18 gm. (59%), m.p. 159°-162°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03961056 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-35e7dfcb8fc44e49a873d439e4db30f9 |
| Source note | uspto-grants-1976_06 |