Cycloheptylamine → HCID 19650470, compound

HRID 1657578Notes

Reaction equation

HRID 1657578 reaction equation
[CH:1]1([N:7]=[C:8]=[S:9])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[CH:10]1([NH2:17])[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11]1.CCOCC>CCCCCC>[CH:10]1([NH:17][C:8]([NH:7][CH:1]2[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]2)=[S:9])[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11]1

Participants

5

Reactant 3

HCID 2899CycloheptylamineHCID 3283Diethyl EtherHCID 14289Cyclohexyl isothiocyanate

Product 1

HCID 19650470HCID 19650470, compound

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

The thiourea is prepared by reacting 14.1 gm. (0.1 mole) of cyclohexyl isothiocyanate and 11.5 gm. (0.1 mole) of cycloheptylamine in 200 ml. of ether for 1.5 hr. at room temperature. Reaction is diluted with an equal volume of Skellysolve B to give 19.5 gm. of product, m.p. 160°-161°.

Workup

  1. customat room temperature
  2. customReaction
  3. customto give 19.5 gm

Sources & evidence

ORD record
ord-5055d17c36864017b3a00dad41681ec4
Source dataset
uspto-grants-1976_06
Patent number
US03961056

Reaction notes

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