HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cycloheptylamine → HCID 19650470, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cycloheptylamine | HCID 2899 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Cyclohexyl isothiocyanate | HCID 14289 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 19650470 | HCID 19650470 | — |
Reaction Steps
The thiourea is prepared by reacting 14.1 gm. (0.1 mole) of cyclohexyl isothiocyanate and 11.5 gm. (0.1 mole) of cycloheptylamine in 200 ml. of ether for 1.5 hr. at room temperature. Reaction is diluted with an equal volume of Skellysolve B to give 19.5 gm. of product, m.p. 160°-161°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03961056 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-5055d17c36864017b3a00dad41681ec4 |
| Source note | uspto-grants-1976_06 |