HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → HCID 54220962, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | Tributylamine | HCID 7622 | — |
| Reactant | HCID 21534896 | HCID 21534896 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 54220962 | HCID 54220962 | — |
Reaction Steps
2.74 g (10 moles) of 1,3-dichloro-4-phenylisoquinoline, 1.02 g (15 mmoles) of imidazole and 2.7 g (15 mmoles) of tri-n-butylamine were heated for 18 hours in 5 ml of dioxane under reflux. Working was carried out as described under 1c.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03961062 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-8bdf5ca1d67049fa8adbd191bbfbb49c |
| Source note | uspto-grants-1976_06 |