HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 21534844, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-Hydroxy-6-dimethylsulphamoylphenothiazine | HCID 21534833 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 21534844 | HCID 21534844 | 45.4% |
Reaction Steps
2-Methoxy-6-dimethylsulphamoylphenothiazine (m.p. 196°-198°C.; 79.6 g.) is prepared by methylation, using dimethyl sulphate (74.5 g.), of 2-hydroxy-6-dimethylsulphamoylphenothiazine (168 g.) in the presence of powdered sodium hydroxide (30.8 g.) suspended in methyl ethyl ketone (1,820 cc.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03961055 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-fdb39b25b8bd48f9a4f95ac4e61fb65c |
| Source note | uspto-grants-1976_06 |