1-Bromo-3-chloropropane → HCID 21534834, compound

HRID 1657592Notes

Reaction equation

HRID 1657592 reaction equation
Br[CH2:2][CH2:3][CH2:4][Cl:5].[CH3:6][O:7][C:8]1[CH:21]=[CH:20][C:19]2[S:18][C:17]3[C:12](=[CH:13][CH:14]=[CH:15][C:16]=3[S:22][CH3:23])[NH:11][C:10]=2[CH:9]=1>>[CH3:6][O:7][C:8]1[CH:21]=[CH:20][C:19]2[S:18][C:17]3[C:12](=[CH:13][CH:14]=[CH:15][C:16]=3[S:22][CH3:23])[N:11]([CH2:2][CH2:3][CH2:4][Cl:5])[C:10]=2[CH:9]=1

Participants

3

Reactant 2

HCID 80061-Bromo-3-chloropropaneHCID 21534831HCID 21534831, compound

Product 1

HCID 21534834HCID 21534834, compoundYield 35.9%

Procedure

2-Methoxy-6-methylthio-10-(3-chloropropyl)-phenothiazine (10.1 g.) is prepared by reacting 1-bromo-3-chloropropane (47.5 g.) with 2-methoxy-6-methylthiophenothiazine (22.0 g.).

Sources & evidence

ORD record
ord-f79018aaa1734b239e50626b444fdbd3
Source dataset
uspto-grants-1976_06
Patent number
US03961055

Reaction notes

Loading…